3-Bromo-4-methylpyridine → HCID 86607580、化合物

反応式

[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([NH:7][C:8]([C:10]2[C:15]([NH:16][C:17]3[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=3)=[CH:14][CH:13]=[C:12]([CH3:23])[N:11]=2)=[O:9])=[N:3]1.Br[C:25]1C=NC=CC=1C>>[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([NH:7][C:8]([C:10]2[C:15]([NH:16][C:17]3[CH:18]=[N:19][CH:20]=[CH:21][C:22]=3[CH3:25])=[CH:14][CH:13]=[C:12]([CH3:23])[N:11]=2)=[O:9])=[N:3]1

参加物

反応物 2

HCID 8176303-Bromo-4-methylpyridine

HCID 11573128HCID 11573128、化合物

生成物 1

HCID 86607580HCID 86607580、化合物

実験手順

The title compound, was prepared from 3-Amino-6-methyl-pyridine-2-carboxylic acid (1-methyl-1H-pyrazol-3-yl)-amide (example 16) in accordance with the general method of example 20 using 3-Bromo-4-methylpyridine instead of 3-Bromo-4-methylpyridine to yield the final compound as a light brown solid, MS (ISP): m/e=323.5 (M+H+).

出典と根拠

ORDレコード: ord-79ba7ad4683242b0bfa54f88f570144a
出典データセット: uspto-grants-2008_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07414060B2

反応ノート

読み込み中…

参加物