3-Bromo-2-methylpyridine → HCID 11573340、化合物

反応式

[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([NH:7][C:8]([C:10]2[C:15]([NH:16][C:17]3[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=3)=[CH:14][CH:13]=[C:12]([CH3:23])[N:11]=2)=[O:9])=[N:3]1.Br[C:25]1C(C)=NC=CC=1>>[CH3:1][N:2]1[CH:6]=[CH:5][C:4]([NH:7][C:8]([C:10]2[C:15]([NH:16][C:17]3[C:18]([CH3:25])=[N:19][CH:20]=[CH:21][CH:22]=3)=[CH:14][CH:13]=[C:12]([CH3:23])[N:11]=2)=[O:9])=[N:3]1

参加物

反応物 2

HCID 12010033-Bromo-2-methylpyridine

HCID 11573128HCID 11573128、化合物

生成物 1

HCID 11573340HCID 11573340、化合物

実験手順

The title compound, was prepared from 3-Amino-6-methyl-pyridine-2-carboxylic acid (1-methyl-1H-pyrazol-3-yl)-amide (example 16) in accordance with the general method of example 20 using 3-Bromo-2-methylpyridine instead of 3-Bromo-4-methylpyridine to yield the final compound as a orange solid, MS (ISP): m/e=323.1 (M+H+).

出典と根拠

ORDレコード: ord-b813f3638e734981bb56d6b72ec24bef
出典データセット: uspto-grants-2008_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07414060B2

反応ノート

読み込み中…