Hydrochloric Acid → HCID 57422604、化合物
反応式
[CH:1]1([C:6]([CH:8]([NH:13]C(=O)OC(C)(C)C)[CH:9]([CH3:12])[CH2:10][CH3:11])=[O:7])[CH2:5][CH2:4][CH2:3][CH2:2]1.[ClH:21]>>[Cl-:21].[CH:1]1([C:6](=[O:7])[CH:8]([NH3+:13])[CH:9]([CH3:12])[CH2:10][CH3:11])[CH2:5][CH2:4][CH2:3][CH2:2]1参加物
3
実験手順
4 (0.18 g, 0.63 mmol) was dissolved in 2 ml HCl (7 N in dioxane). After completion of the reaction the solvent was removed and the resulting oil was purified by column chromatography on silical gel using a chloroform/methanol/water gradient. The resulting oil was triturated with ether.
後処理
- customAfter completion of the reaction the solvent
- customwas removed
- customthe resulting oil was purified by column chromatography on silical gel
- customThe resulting oil was triturated with ether
出典と根拠
- ORDレコード
- ord-5f226638af4a4721ae8f6021d80ee866
- 出典データセット
- uspto-grants-2008_05
- 特許番号
- US07368421B2
反応ノート
読み込み中…