化工社化工社 化学情報印刷レポート · 研究参考用
Methanethiol → N-acetyl-L-methionine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanethiol | HCID 878 | — |
| 反応物 | N-(2-oxooxolan-3-yl)acetamide | HCID 325257 | — |
| 生成物 | N-acetyl-L-methionine | HCID 448580 | — |
反応手順
Subsequently the N-acetyl-2-aminobutyrolactone (1 eq) was reacted with various bases in MeSH to give N-acetylmethionine. A mixture of N-acetylaminolactone, base and MeSH (14 eq) was heated in a sealed autoclave. After cooling, expansion and removal of MeSH, the remaining oil was analysed by HPLC. Further details and the yield of N-acetyl-L-methionine achieved are listed in the table below:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07368600B2 |
| 出典データセット | uspto-grants-2008_05 |
| ORD ID | ord-3eaa024cf8064eb6ab1f1ef13ef8f70a |
| 出典メモ | uspto-grants-2008_05 |