Dipentylamine → HCID 178446345、化合物

HRID 2222081

反応式

HRID 2222081 の反応式
[I-:1].[I-].[I-].[CH2:4]([N:7]([C:11]1[CH:12]=[CH:13][C:14]2[C:23]([CH:24]=1)=[S+:22][C:21]1[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=1)[N:15]=2)[CH2:8][CH2:9][CH3:10])[CH2:5][CH3:6].C(N([C:32]1[CH:33]=[CH:34][C:35]2C([CH:45]=1)=[S+]C1[C:37](=[CH:38][CH:39]=[CH:40][CH:41]=1)[N:36]=2)CCC)CC.C(N(C1C=CC2C(C=1)=[S+]C1C(=CC=CC=1)N=2)CCC)CC.C(NCCCCC)CCCC>>[I-:1].[CH2:37]([N:36]([C:19]1[CH:18]=[CH:17][C:16]2[C:21]([CH:20]=1)=[S+:22][C:23]1[C:14](=[CH:13][CH:12]=[C:11]([N:7]([CH2:8][CH2:9][CH3:10])[CH2:4][CH2:5][CH3:6])[CH:24]=1)[N:15]=2)[CH2:35][CH2:34][CH2:33][CH2:32][CH3:45])[CH2:38][CH2:39][CH2:40][CH3:41]

参加物

3

反応物 2

HCID 16316DipentylamineHCID 178457153HCID 178457153、化合物

生成物 1

HCID 178446345HCID 178446345、化合物

実験手順

This compound was obtained following isolation of 3-(N,N-dipropylamino)-phenothiazin-5-ium triiodide and subsequent treatment with dipentylamine. Precipitation from dichloromethane by addition of diethyl ether yielded purple lustrous crystals. Mass spectrometry: C28H42N3OS requires m/z=452; found m/z=452 (I− not detected by mass spectrometry).

後処理

  1. customThis compound was obtained
  2. customPrecipitation from dichloromethane
  3. additionby addition of diethyl ether yielded purple lustrous crystals

出典と根拠

ORDレコード
ord-5235de8511c244119ac2aa6d8ed2459b
出典データセット
uspto-grants-2008_05
特許番号
US07371744B2

関連ノート

読み込み中…