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Benzene, 1-chloro-3-isocyanato- → 1-(3-Chlorophenylcarbamoyl)-2-nitroiminoimidazolidine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzene, 1-chloro-3-isocyanato- | HCID 17968 | — |
| 反応物 | N-nitroimidazolidin-2-imine | HCID 135413413 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 1-(3-Chlorophenylcarbamoyl)-2-nitroiminoimidazolidine | HCID 136342791 | — |
反応手順
A solution of 3.9 g of 2-nitroiminoimidazolidine and 4.6 g of 3-chlorophenylisocyanate in 80 ml of dry acetonitrile was refluxed for 3 hours. After cooling to room temperature, the precipitated crystals were filtered, and washed with ether to give desired 1-(3-chlorophenylcarbamoyl)-2-nitroiminoimidazolidine. The yield was 4.7 g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05428032 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-0c6503fe8c694880a74608b8a801c8d1 |
| 出典メモ | uspto-grants-1995_06 |