3-(4-Methylpiperazine-1-sulfonyl)aniline → HCID 69293088、化合物
反応式
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[C:12]([CH:14]([F:16])[F:15])[N:11]3[N:17]=[CH:18][C:19]([C:20](O)=[O:21])=[C:10]3[N:9]=2)=[CH:4][CH:3]=1.[CH3:23][N:24]1[CH2:29][CH2:28][N:27]([S:30]([C:33]2[CH:34]=[C:35]([NH2:39])[CH:36]=[CH:37][CH:38]=2)(=[O:32])=[O:31])[CH2:26][CH2:25]1>>[CH3:23][N:24]1[CH2:29][CH2:28][N:27]([S:30]([C:33]2[CH:34]=[C:35]([NH:39][C:20]([C:19]3[CH:18]=[N:17][N:11]4[C:12]([CH:14]([F:15])[F:16])=[CH:13][C:8]([C:5]5[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=5)=[N:9][C:10]=34)=[O:21])[CH:36]=[CH:37][CH:38]=2)(=[O:32])=[O:31])[CH2:26][CH2:25]1参加物
3
実験手順
The title compound was prepared from 5-(4-chloro-phenyl)-7-difluoromethyl-pyrazolo[1,5-a]pyrimidine-3-carboxylic acid (example C.3) and 3-(4-methyl-piperazine-1-sulfonyl)-phenylamine [CAS 436095-35-1] according to general procedure II. Yellow solid. MS (ISP) 561.5 [(M+H)+]; mp 147° C.
出典と根拠
- ORDレコード
- ord-c72154cd68ad492abd9a0fa1adefdeb4
- 出典データセット
- uspto-grants-2008_05