3-Aminophenyl trifluoromethyl sulfone → HCID 11585073、化合物
反応式
[F:1][C:2]([F:26])([F:25])[C:3]1[N:8]2[N:9]=[CH:10][C:11]([C:12](O)=[O:13])=[C:7]2[N:6]=[C:5]([C:15]2[CH:20]=[CH:19][C:18]([C:21]([F:24])([F:23])[F:22])=[CH:17][CH:16]=2)[CH:4]=1.[F:27][C:28]([F:40])([F:39])[S:29]([C:32]1[CH:33]=[C:34]([NH2:38])[CH:35]=[CH:36][CH:37]=1)(=[O:31])=[O:30]>>[F:40][C:28]([F:39])([F:27])[S:29]([C:32]1[CH:33]=[C:34]([NH:38][C:12]([C:11]2[CH:10]=[N:9][N:8]3[C:3]([C:2]([F:26])([F:25])[F:1])=[CH:4][C:5]([C:15]4[CH:20]=[CH:19][C:18]([C:21]([F:24])([F:22])[F:23])=[CH:17][CH:16]=4)=[N:6][C:7]=23)=[O:13])[CH:35]=[CH:36][CH:37]=1)(=[O:30])=[O:31]参加物
3
実験手順
The title compound was prepared from 7-trifluoromethyl-5-(4-trifluoromethyl-phenyl)-pyrazolo[1,5-a]pyrimidine-3-carboxylic acid (example C.2) and 3-trifluoromethanesulfonyl-phenylamine [commercially available] according to general procedure II. Yellow solid. MS (ISP) 583.3 [(M+H)+]; mp 207° C.
出典と根拠
- ORDレコード
- ord-a3a59235241240f784d269baa2a499bd
- 出典データセット
- uspto-grants-2008_05