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(4S)-4-{[(benzyloxy)carbonyl]amino}-5-methoxy-5-oxopentanoic acid → Z-Glu-Ala-Ala-OH
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (4S)-4-{[(benzyloxy)carbonyl]amino}-5-methoxy-5-oxopentanoic acid | HCID 2733408 | — |
| 反応物 | L-Alanyl-L-alanine | HCID 5484352 | — |
| 生成物 | Z-Glu-Ala-Ala-OH | HCID 15730994 | — |
反応手順
0.2 ml of aqueous solution containing 2 mM Z-Glu-OMe, 50 mMH-Ala-Ala-OH, 25 mMNaOH and 5 mg/ml endoproteinase Glu-C are deep-frozen. Subsequently the reaction mixture is kept at -25° C. until the Z-Glu-OMe is consumed. Following thawing, the yield is determined analytically by RP-HPLC and amounts to 76% of theory.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05350682 |
| 出典データセット | uspto-grants-1994_09 |
| ORD ID | ord-fa470512c0aa482a82c110ca6bb61832 |
| 出典メモ | uspto-grants-1994_09 |