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Formic Acid → 3-(3,4-Dimethoxyphenyl)propionic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | Veratraldehyde | HCID 8419 | — |
| 反応物 | 2-(4-Fluorophenyl)-1,3-dioxane-4,6-dione | HCID 19938682 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 3-(3,4-Dimethoxyphenyl)propionic acid | HCID 75019 | — |
反応手順
5.26 g (0.025 mol) of 2-(4-fluorophenyl)-1,3-dioxane-4,6-dione (m.p.: 166°-167° C.) and 4.15 g (0.025 mol) of veratraldehyde were added to 25 ml of the mixture of formic acid and triethylamine prepared as described in Example 1. The reaction was carried out according to Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05350872 |
| 出典データセット | uspto-grants-1994_09 |
| ORD ID | ord-93ad8b5c70aa4baeb0248dd498d8ee07 |
| 出典メモ | uspto-grants-1994_09 |