化工社化工社 化学情報印刷レポート · 研究参考用
Formic Acid → 3,4,5-Trimethoxyhydrocinnamic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Formic Acid | HCID 284 | — |
| 反応物 | 2,2-Dimethyl-5-(3,4,5-trimethoxybenzylidene)-1,3-dioxane-4,6-dione | HCID 370323 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | 3,4,5-Trimethoxyhydrocinnamic acid | HCID 64860 | — |
反応手順
16.1 g (0.05 mol) of 5-(3,4,5-trimethoxyphenylmethylene)- 2,2-dimethyl-1,3-dioxane-4,6-dione (m.p.: 159°-160° C.) were added to 50 ml of the mixture of formic acid and triethylamine prepared as described in Example 1, then the procedure described in Example 2 was followed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05350872 |
| 出典データセット | uspto-grants-1994_09 |
| ORD ID | ord-bce13e3f60fe453781907d2d7b290140 |
| 出典メモ | uspto-grants-1994_09 |