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Benzenamine, 4-(4-fluorophenoxy)- → [4-(4-Fluoro-phenoxy)-phenyl]-(2-methyl-6-nitro-phenyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzenamine, 4-(4-fluorophenoxy)- | HCID 147633 | — |
| 反応物 | 2-Fluoro-1-methyl-3-nitrobenzene | HCID 13470957 | — |
| 反応物 | Potassium tert-butoxide | HCID 23665647 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | [4-(4-Fluoro-phenoxy)-phenyl]-(2-methyl-6-nitro-phenyl)-amine | HCID 68837567 | — |
反応手順
The product (790 mg) is obtained according to the method of stage 1 of Example 4, by using 900 μL of 2-fluoro-3-methyl-nitrobenzene and 2.6 g of 4-(4-fluoro-phenoxy)-phenylamine obtained in stage 2 of Example 5 in the presence of 2.36 g of potassium tert-butanolate in 80 mL of DMSO.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08207373B2 |
| 出典データセット | uspto-grants-2012_06 |
| ORD ID | ord-23473f25389845a294d96dba157a51d1 |
| 出典メモ | uspto-grants-2012_06 |