化工社化工社 化学情報印刷レポート · 研究参考用
Benzenamine, 4-(phenylmethyl)- → (4-Benzyl-phenyl)-(2-methyl-6-nitro-phenyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzenamine, 4-(phenylmethyl)- | HCID 136914 | — |
| 反応物 | 2-Fluoro-1-methyl-3-nitrobenzene | HCID 13470957 | — |
| 反応物 | Potassium tert-butoxide | HCID 23665647 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | (4-Benzyl-phenyl)-(2-methyl-6-nitro-phenyl)-amine | HCID 68834454 | — |
反応手順
The product (1.01 g) is obtained according to the method of stage 1 of Example 4, by using 1.13 g of 2-fluoro-3-methyl-nitrobenzene and 2 g of 4-benzyl-aniline in the presence of 1.31 g of potassium tert-butanolate in 30 mL of DMSO.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08207373B2 |
| 出典データセット | uspto-grants-2012_06 |
| ORD ID | ord-d458c972e6344078914415d4be3fddfb |
| 出典メモ | uspto-grants-2012_06 |