関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Palmitic Acid | HCID 985 | — |
| 反応物 | Stearic Acid | HCID 5281 | — |
| 反応物 | Zinc Hydroxide | HCID 9812759 | — |
| 生成物 | Palmitic Acid | HCID 985 | — |
| 生成物 | Zinc Stearate | HCID 11178 | — |
反応手順
Stearic acid and palmitic acid were mixed at a mass ratio of 65:35 to prepare a mixture, and zinc hydroxide was mixed and melted with the resulting mixture to be reacted therewith, and then dried to produce particles in which zinc stearate and palmitic acid were dissolved in each other (particle diameter: 11 μm to 23 μm). A part of the particles thus produced was dissolved in a hydrochloric acid-methanol solution, and the product was heated to 80° C. to methylate the stearic acid and palmitic acid. The methylation product was analyzed by gas chromatography to determine the zinc stearate content and the palmitic acid content and to express them in terms of the equivalent ratio of zinc stearate to zinc palmitate, and the ratio was found to be 64:34 (mass ratio).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US08208835B2 |
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| 出典データセット | uspto-grants-2012_06 |
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| ORD ID | ord-d1459e51b4364b2ea630ff8db1e31bf3 |
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| 出典メモ | uspto-grants-2012_06 |
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