化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → N-(2,4,6-tribromophenyl)glycinamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | Bromine | HCID 24408 | — |
| 反応物 | N-Phenylglycine ethyl ester | HCID 75190 | — |
| 反応物 | ethyl N-(2,4,6-tribromophenyl)glycinate | HCID 12659467 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | N-(2,4,6-tribromophenyl)glycinamide | HCID 28992175 | — |
反応手順
The ester required for Id, ethyl N-(2,4,6-tribromophenyl)glycinate (IV), was prepared by the reaction of ethyl N-phenylglycinate with bromine in a mixture of water and acetic acid. IV reacted with ammonia in ethanol solution to form N-(2,4,6-tribromophenyl)glycinamide (V).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04352930 |
| 出典データセット | uspto-grants-1982_10 |
| ORD ID | ord-12a572969296471cbfd69e364352926a |
| 出典メモ | uspto-grants-1982_10 |