Triethylamine → HCID 21920917、化合物
反応式
[NH2:1][CH:2]1[CH2:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][C:8]=2[CH3:11])[CH2:3]1.C(N(CC)CC)C.[F:19][C:20]1[CH:28]=[CH:27][C:23]([C:24](Cl)=[O:25])=[CH:22][CH:21]=1>O1CCOCC1>[F:19][C:20]1[CH:28]=[CH:27][C:23]([C:24]([NH:1][CH:2]2[CH2:10][C:9]3[C:4](=[CH:5][CH:6]=[CH:7][C:8]=3[CH3:11])[CH2:3]2)=[O:25])=[CH:22][CH:21]=1参加物
5
実験手順
370 mg (2.52 mmol) 2-amino-4-methylindane and 257 mg (2.52 mmol) triethylamine were dissolved in 5 ml dioxane, 400 mg (2.52 mmol) 4-fluorobenzoylchloride were added, and the mixture was stirred for 2 h at room temperature (RT).
出典と根拠
- ORDレコード
- ord-9c91932c5f2e45f196fcb05d1a288e99
- 出典データセット
- uspto-grants-2010_05
- 特許番号
- US07713963B2
反応ノート
読み込み中…