関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
| 反応物 | Benzoin ethyl ether | HCID 101778 | — |
| 反応物 | Diisocyanatotoluene | HCID 12905475 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Adipic Acid | HCID 196 | — |
| 生成物 | Phthalic Acid | HCID 1017 | — |
| 生成物 | Trimethylolpropane | HCID 6510 | — |
反応手順
1.2 A 12% strength solution of a mixture of 2 parts of benzoin ethyl ether, 6 parts of the reaction product of 1 mole of toluylene diisocyanate and 2 moles of β-hydroxyethyl methacrylate and 92 parts of the polyvinyl alcohol/methacrylic anhydride reaction product, prepared as described in 1.1, in a mixture of equal parts of water and ethanol is prepared. The solution is applied to a steel sheet which has been coated with a polyurethane adhesive according to German Laid-Open Application DOS No. 1,597,515 (prepared from a commercial hydroxy-containing polyester, obtained from 2.5 moles of adipic acid, 0.5 mole of phthalic acid and 4 moles of 1,1,1-trimethylolpropane, by reaction with a triisocyanate prepared by reacting 3 moles of toluylene diisocyanate with 1 mole of 1,1,1-trimethylolpropane), the amount of solution applied to the sheet being such that, after curing for 7 minutes in a cabinet dryer at 150° C., a 10 μm thick intermediate layer (c) results.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04355093 |
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| 出典データセット | uspto-grants-1982_10 |
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| ORD ID | ord-3a9014de7a3646218300cd7665d36f73 |
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| 出典メモ | uspto-grants-1982_10 |
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