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HRID 2236389作成日:2026年10月27日

Piperonal → Bis(3,4-methylenedioxy)chalcone

https://huagongshe.com/reaction/2236389

反応式

関与物質

役割名称HCID仕込み量
反応物PiperonalHCID 8438—
反応物Sodium HydroxideHCID 14798—
反応物AcetopiperoneHCID 76622—
溶媒EthanolHCID 702—
生成物Bis(3,4-methylenedioxy)chalconeHCID 294346—

反応手順

A mixture of piperonal (460 mg) and 3,4-methylenedioxyacetophenone (500 mg) in ethanol (20 ml) was treated with 1M NaOH solution (4 ml), then the mixture was stirred overnight. The pale yellow crystalline solid was filtered off, washed with water then cold aqueous ethanol and dried to give pure bis(3,4-methylenedioxy)chalcone DC-0006B (476 mg, 53%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07714170B2
出典データセットuspto-grants-2010_05
ORD IDord-ce87f20780d94c05ae7f530b9f8236b0
出典メモuspto-grants-2010_05