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Hydrochloric Acid → 2-Ethyl-2-n-butyl-11-phenyl-11-amino-undeca-4,8-dienal-oxime
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 反応物 | 3-Ethyl-3-n-butyl-12-phenyl-1-aza-1,5,9-cyclododecatriene | HCID 54523241 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 2-Ethyl-2-n-butyl-11-phenyl-11-amino-undeca-4,8-dienal-oxime | HCID 73678919 | 100% |
反応手順
The procedure described in Example 1(b) is repeated, except that 283.4 g (0.875 mol) of 3-n-butyl-3-ethyl-12-phenyl-1-aza-1,5,9-cyclododecatriene, 60.8 g (0.87 mol) of hydroxylamine hydrochloride, 50 ml of concentrated hydrochloric acid and 250 ml of water are used. Working up yields 310 g (0.87 mol) of 2-n-butyl-2-ethyl-11-phenyl-11-amino-undeca-4,8-dienal oxime; yield 99.5% of theory.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04355177 |
| 出典データセット | uspto-grants-1982_10 |
| ORD ID | ord-811b847bcc4049f289519692750ea915 |
| 出典メモ | uspto-grants-1982_10 |