4-Chloromethyl-2-methoxy-biphenyl → 1-Butyl-4-chloromethyl-2-methoxy-benzene

反応式

[Cl:1][CH2:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2C=C[CH:12]=[CH:11][CH:10]=2)=[C:5]([O:15][CH3:16])[CH:4]=1.C(C1C=CC(CO)=CC=1OC)CCC>>[CH2:9]([C:6]1[CH:7]=[CH:8][C:3]([CH2:2][Cl:1])=[CH:4][C:5]=1[O:15][CH3:16])[CH2:10][CH2:11][CH3:12]

参加物

反応物 2

HCID 593001244-Chloromethyl-2-methoxy-biphenyl

HCID 59300341(4-Butyl-3-methoxy-phenyl)-methanol

生成物 1

HCID 593002161-Butyl-4-chloromethyl-2-methoxy-benzene

実験手順

Following the same procedure for the preparation of 4-Chloromethyl-2-methoxy-biphenyl, the title compound is prepared from (4-Butyl-3-methoxy-phenyl)-methanol (crude material from the previous step). The crude material is used directly in the next step.

出典と根拠

ORDレコード: ord-39c36ffb60c044b4abf34ee7d106765f
出典データセット: uspto-grants-2010_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07713994B2

反応ノート

読み込み中…