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Hydrochloric Acid → 2,2-Dimethyl-11-isopropyl-11-amino-undeca-4,8-dienal semicarbazone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Semicarbazide hydrochloride | HCID 11236 | — |
| 反応物 | 3,3-Dimethyl-12-isopropyl-1-aza-1,5,9-cyclododecatriene | HCID 557512 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 2,2-Dimethyl-11-isopropyl-11-amino-undeca-4,8-dienal semicarbazone | HCID 54254998 | 86% |
反応手順
The procedure described in Example 1(b) is repeated, except that 23.3 g (0.1 mol) of 3,3-dimethyl-12-isopropyl-1-aza-1,5,9-cyclododecatriene, 20 g of 37% hydrochloric acid, 20 ml of water and 11.15 g (0.1 mol) of semicarbazide hydrochloride are used. Working up yields 26.5 g (0.086 mol) of 2,2-dimethyl-11-isopropyl-11-amino-undeca-4,8-dienal semicarbazone; yield 86% of theory.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04355177 |
| 出典データセット | uspto-grants-1982_10 |
| ORD ID | ord-9aa670777b5f407bba7fb02256f2d00a |
| 出典メモ | uspto-grants-1982_10 |