関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Ethyl p-methylbenzenesulfonate | HCID 6638 | — |
| 反応物 | 1,3-benzoxazole-2-thiol | HCID 178418282 | — |
| 生成物 | 2-Ethylmercapto-3-ethylbenzoxazolium p-toluenesulfonate | HCID 86738611 | — |
反応手順
A mixture of 3.0 g of 2-mercaptobenzoxazole and 12.0 g of ethyl p-toluenesulfonate was heated to 150° C. to react them for 6 hours. The reaction product was cooled to 80° C., and 25 ml of ethanol was added to it, thereby producing an ethanol solution of 2-ethylmercapto-3-ethylbenzoxazolium-p-toluenesulfonate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04356247 |
|---|
| 出典データセット | uspto-grants-1982_10 |
|---|
| ORD ID | ord-6d3676ef55cf40839f114250a86a744b |
|---|
| 出典メモ | uspto-grants-1982_10 |
|---|
