Sodium Dimethyldithiocarbamate → Ziram

HRID 223766

反応式

HRID 223766 の反応式
[CH3:1][N:2]([C:4]([S-:6])=[S:5])[CH3:3].[Na+].[Cl-].[Cl-].[Zn+2:10]>O>[CH3:1][N:2]([C:4]([S-:6])=[S:5])[CH3:3].[CH3:1][N:2]([C:4]([S-:6])=[S:5])[CH3:3].[Zn+2:10]

参加物

4

反応物 2

HCID 560256Sodium Dimethyldithiocarbamate2 回HCID 3007855Zincchloride

生成物 1

HCID 8722Ziram

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Sodium dimethyl dithiocarbamate (75.2 g, 0.66 mole) is dissolved in 100 ml H2O. A ZnCl2 solution (45.4 g, 0.33 mole dissolved in 300 ml H2O) is added to the sodium dimethyl dithiocarbamate solution. Immediately, a white precipitate forms which is filtered and dried to give a quantitative yield of zinc dimethyl dithiocarbamate.

後処理

  1. filtrationImmediately, a white precipitate forms which is filtered
  2. customdried

出典と根拠

ORDレコード
ord-8f902aa3dd244ca4a0b3712670d646a1
出典データセット
uspto-grants-1982_10
特許番号
US04356274

関連ノート

読み込み中…