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Potassium Hydroxide → HCID 20520763、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 1-Iododecane | HCID 16314 | — |
| 反応物 | 1-Iodododecane | HCID 20282 | — |
| 反応物 | 2-(1H-imidazol-2-yl)pyridine | HCID 589313 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | HCID 20520763 | HCID 20520763 | 103.7% |
反応手順
A mixture of 14.5 g (0.1 mole) 2-(2-pyridyl)imidazole, 6 g (0.11 mole) ground KOH, 30 g (0.1 mole) iodododecane in about 150 ml of acetonitrile was stirred and refluxed for about 2 hours. The iododecane gradually went into solution as the reaction proceeded. After the 2 hours the reaction mixture was cooled and filtered. The resulting residue was extracted with hexane to give 32.5 g of crude product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04356309 |
| 出典データセット | uspto-grants-1982_10 |
| ORD ID | ord-71aaab8d01e14499bd40051edaaf5053 |
| 出典メモ | uspto-grants-1982_10 |