化工社化工社 化学情報印刷レポート · 研究参考用
Triethyl Citrate → Ethyl Acetoacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethyl Citrate | HCID 6506 | — |
| 触媒 | Titanium isopropoxide | HCID 11026 | — |
| 生成物 | Ethyl Acetoacetate | HCID 8868 | — |
反応手順
In the same way as in Example 1, 60 g (0.21 mol) of tetraisopropyl titanate were reacted with 116.6 g (0.42 mol) of triethyl citrate. The mixture was freed of alcohol under vacuum and 154.6 g of a clear, pale yellow liquid was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05428103 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-0b1f2e1c0f294ff991c72bb3ca95134c |
| 出典メモ | uspto-grants-1995_06 |