Benzene → 2,3-Dimethyl-5-allyl-6-tetradecanoylhydroquinone

HRID 224469ノート

反応式

HRID 224469 の反応式
C([O:4][C:5]1[C:10]([C:11](=[O:25])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])=[CH:9][C:8]([OH:26])=[C:7]([CH3:27])[C:6]=1[CH3:28])C=C.[CH:29]1[CH:34]=CC=C[CH:30]=1>>[CH3:28][C:6]1[C:7]([CH3:27])=[C:8]([OH:26])[C:9]([CH2:34][CH:29]=[CH2:30])=[C:10]([C:11](=[O:25])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[C:5]=1[OH:4]

参加物

3

反応物 2

HCID 241BenzeneHCID 233332484-Hydroxy-2,3-dimethyl-6-tetradecanoylphenyl allyl ether

生成物 1

HCID 205104582,3-Dimethyl-5-allyl-6-tetradecanoylhydroquinone

実験手順

90 g of the allyl ether of step 2 were heated to 210° C. under nitrogen atmosphere within 2 h. After cooling the melt was dissolved in 300 ml of benzine (boiling range: 50°-75° C.) and placed in a cool place. The precipitate formed was filtered with suction the next day.

後処理

  1. temperatureAfter cooling the melt
  2. customThe precipitate formed
  3. filtrationwas filtered with suction the next day

出典と根拠

ORDレコード
ord-7c05fbbb7b284f8d945e48ff232f998e
出典データセット
uspto-grants-1980_11
特許番号
US04232107

反応ノート

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