化工社化工社 化学情報印刷レポート · 研究参考用
Hydrogen Sulfide → 1-Dodecanethiol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Sulfide | HCID 402 | — |
| 反応物 | 1-Dodecene | HCID 8183 | — |
| 溶媒 | Diglyme | HCID 8150 | — |
| 生成物 | 1-Dodecanethiol | HCID 8195 | — |
反応手順
Under the conditions of Example 3, with an input of 38 liters per hour of hydrogen sulphide, 67.7 mmoles of dodecene-1 dissolved in diglyme at a concentration of 0.564 mole per liter were irradiated at 11° C. After 3 minutes of irradiation, 48.2 mmoles of n-dodecyl mercaptan were formed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04233128 |
| 出典データセット | uspto-grants-1980_11 |
| ORD ID | ord-b779b01eec7b4804ae0da5ef95b9639e |
| 出典メモ | uspto-grants-1980_11 |