化工社化工社 化学情報印刷レポート · 研究参考用
5,6-Diamino-3-methyl-1-phenyluracil → 3,7-dihydro-1-methyl-3-phenyl-8-propyl-1H-purine-2,6-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5,6-Diamino-3-methyl-1-phenyluracil | HCID 11075275 | — |
| 溶媒 | Butyric anhydride | HCID 7798 | — |
| 生成物 | 3,7-dihydro-1-methyl-3-phenyl-8-propyl-1H-purine-2,6-dione | HCID 23331678 | — |
反応手順
A solution of 3 g of 5,6-diamino-3-methyl-1-phenyl-2,4-(1H, 3H)-pyrimidinedione XVIII in 25 ml of butyric anhydride was refluxed for 16 hours. After cooling, grey crystals were filtered off and recrystallized from 100 ml of ethanol. Yield 1.1 g NMR.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04233303 |
| 出典データセット | uspto-grants-1980_11 |
| ORD ID | ord-7bb604bf4dae465d9037e14ba509730b |
| 出典メモ | uspto-grants-1980_11 |