関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydroxylamine | HCID 787 | — |
| 反応物 | N-(3-chloro-4-cyanophenyl)methanesulfonamide | HCID 669685 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 2-Chloro-N'-hydroxy-4-[(methylsulfonyl)amino]benzenecarboximidamide | HCID 72533799 | — |
反応手順
To a stirred solution of the product from Step A (0.13 g, 0.565 mmol) in ethanol (3 mL) was added hydroxylamine (50% in water, 1.0 mL). The reaction was heated at 90° C. for 2 h. The reaction was then concentrated to give the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07687492B2 |
|---|
| 出典データセット | uspto-grants-2010_03 |
|---|
| ORD ID | ord-29c660b8b31b4cfb89eb3c7c518f418c |
|---|
| 出典メモ | uspto-grants-2010_03 |
|---|
