化工社化工社 化学情報印刷レポート · 研究参考用
Octylamine → N-Heptyl-N'-octylthiourea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Octylamine | HCID 8143 | — |
| 反応物 | Heptane, 1-isothiocyanato- | HCID 78152 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | N-Heptyl-N'-octylthiourea | HCID 12796254 | 105.2% |
反応手順
To a solution of 3.14 grams (0.02 mole) n-heptylisothiocyanate dissolved in 15 milliliters of benzene is added 2.58 grams (0.02 mole) n-octylamine. The temperature rose to 41° C. The mixture was then refluxed on a steam-bath for about 20 minutes, until the mixture reached a neutral pH. The solution was then evaporated under vacuum. A yield of 6.03 grams of 1-n-heptyl-3-n-octylthiourea was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04233318 |
| 出典データセット | uspto-grants-1980_11 |
| ORD ID | ord-738f6d1da8e247faab1b64ec6a9fbdaf |
| 出典メモ | uspto-grants-1980_11 |