Phenol → Phenylthionophosphonic dichloride
反応式
[C:1]1(O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[P:8](Cl)([Cl:11])([Cl:10])=[S:9]>>[C:1]1([P:8]([Cl:11])([Cl:10])=[S:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1参加物
3
実験手順
Phenol is treated with an excess of thiophosphoryl chloride (at reflux) to yield phenyl thiophosphoryl dichloride ##STR16## and this product was condensed with p-nitroaniline and hydrogenated as set out in Example 1. The corresponding polymer is obtained by polycondensation with isophthaloyl chloride as in Example 2. The inherent viscosity was 0.9 dl/g.
出典と根拠
- ORDレコード
- ord-f44c1da95ea34092b1ab383132191d1c
- 出典データセット
- uspto-grants-1980_11
- 特許番号
- US04233434
反応ノート
読み込み中…