関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Methyl-4-amino-5-aminomethylpyrimidine carbonate | HCID 17991879 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | 4-Amino-2-methyl-5-pyrimidinemethanamine | HCID 66762 | — |
反応手順
An amount of 170 g of isopropanol was added to 30.0 g of the 2-methyl-4-amino-5-aminomethylpyrimidine carbonate thus obtained, followed by heating at about 85° C. for 180 minutes to give 2-methyl-4-amino-5-aminomethylpyrimidine with purity of 99.0%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05037982 |
|---|
| 出典データセット | uspto-grants-1991_08 |
|---|
| ORD ID | ord-a50f703487d34e34a96e06a641c77b92 |
|---|
| 出典メモ | uspto-grants-1991_08 |
|---|
