Methanol → Methyl 3-hydroxy-4-methyl-5-methoxythiophene-2-carboxylate
反応式
Cl[C:2]1([C:9]([O:11][CH3:12])=[O:10])[C:6](=[O:7])[C:5]([CH3:8])=[CH:4][S:3]1.[CH3:13][OH:14]>>[OH:7][C:6]1[C:5]([CH3:8])=[C:4]([O:14][CH3:13])[S:3][C:2]=1[C:9]([O:11][CH3:12])=[O:10]参加物
3
実験手順
The product of (d) above (3 g) was dissolved in 15 ml of methanol and stirred 8 hours at room temperature. The precipitate was filtered and recrystallised from methanol, m.p. 63°-65° C.
後処理
- filtrationThe precipitate was filtered
- customrecrystallised from methanol, m.p. 63°-65° C.
出典と根拠
- ORDレコード
- ord-295e2efad9a74dfe90703e0c11c85f6c
- 出典データセット
- uspto-grants-1991_08
- 特許番号
- US05041461
反応ノート
読み込み中…