2-Chlorobenzenesulfonamide → HCID 57020800、化合物

HRID 2248785

反応式

HRID 2248785 の反応式
[CH3:1][N:2]([CH3:31])[C:3](=[O:30])[NH:4][CH:5]([CH3:29])[CH2:6][C:7]1[CH:8]=[C:9]2[C:13](=[CH:14][CH:15]=1)[N:12]([CH3:16])[CH:11]=[C:10]2[CH2:17][C:18]1[CH:26]=[CH:25][C:21]([C:22](O)=[O:23])=[CH:20][C:19]=1[O:27][CH3:28].[Cl:32][C:33]1[CH:38]=[CH:37][CH:36]=[CH:35][C:34]=1[S:39]([NH2:42])(=[O:41])=[O:40]>>[CH3:31][N:2]([CH3:1])[C:3](=[O:30])[NH:4][CH:5]([CH3:29])[CH2:6][C:7]1[CH:8]=[C:9]2[C:13](=[CH:14][CH:15]=1)[N:12]([CH3:16])[CH:11]=[C:10]2[CH2:17][C:18]1[CH:26]=[CH:25][C:21]([C:22]([NH:42][S:39]([C:34]2[CH:35]=[CH:36][CH:37]=[CH:38][C:33]=2[Cl:32])(=[O:41])=[O:40])=[O:23])=[CH:20][C:19]=1[O:27][CH3:28]

参加物

3

反応物 2

HCID 814102-ChlorobenzenesulfonamideHCID 571952834-[5-[2-(N',N'-dimethylureido)propyl]-1-methylindol-3-ylmethyl]-3-methoxybenzoic acid

生成物 1

HCID 57020800HCID 57020800、化合物

実験手順

Using a similar procedure to that described in Example 2, part c, except starting from 4-[5-[2-(N',N'-dimethylureido)propyl]-1-methylindol-3-ylmethyl]- 3-methoxybenzoic acid, and using 2-chlorophenylsulfonamide instead of 2-methylphenylsulfonamide, the title compound was obtained (88%) as a white solid; mp 131°-136° C.

出典と根拠

ORDレコード
ord-b7475bf950634a30a2c723532b5a469b
出典データセット
uspto-grants-1991_08
特許番号
US05041460

関連ノート

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