Methanol → HCID 14133519、化合物
反応式
[CH3:1][O:2][C:3](=[O:6])[CH2:4]Br.[O-:7][C:8]#[N:9].[K+].[CH3:11][OH:12]>CN(C=O)C>[CH3:1][O:2][C:3](=[O:6])[CH2:4][NH:9][C:8]([O:12][CH3:11])=[O:7]参加物
5
実験手順
10.71 grams of monobromo acetic acid methyl ester, 8.52 grams of potassium cyanate and 7.85 grams of methanol were heated in 70 ml of DMF following the procedure of Example 1 gave 6.62 grams (64.3%) of methoxycarbonylamino acetic acid methyl ester having a boiling point of 67°-8° C./0.0013 mbar.
出典と根拠
- ORDレコード
- ord-05549a776bd743fbaa64dcd7bca35360
- 出典データセット
- uspto-grants-1980_11
- 特許番号
- US04234744
反応ノート
読み込み中…