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4-tert-Butylbenzaldehyde → 4-tert-Butyltoluene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-tert-Butylbenzaldehyde | HCID 70324 | — |
| 反応物 | Benzenemethanol, 4-(1,1-dimethylethyl)-, 1-acetate | HCID 105421 | — |
| 生成物 | 4-tert-Butyltoluene | HCID 7390 | 75.5% |
反応手順
If the material discharged from the electrolysis is worked up similarly to Example 1, 120.3 g of p-tert.-butylbenzaldehyde and 144.1 g of p-tert.-butylbenzyl acetate are obtained in addition to 13.2 g of unconverted p-tert.-butyltoluene. This corresponds to a yield of 75.5% and a current efficiency of 51.4%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04235683 |
| 出典データセット | uspto-grants-1980_11 |
| ORD ID | ord-76e1802c3b4544c49b9d843b0e1ae3a0 |
| 出典メモ | uspto-grants-1980_11 |