Myristic Acid → Tetradecanoic acid, strontium salt (2:1)

HRID 225034

反応式

HRID 225034 の反応式
[C:1]([OH:16])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].O.O.O.O.O.O.O.O.[OH-].[Sr+2:26].[OH-]>O>[C:1]([O-:16])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[Sr+2:26].[C:1]([O-:16])(=[O:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]

参加物

4

反応物 2

HCID 11005Myristic AcidHCID 21617461Strontium hydroxide octahydrate

生成物 1

HCID 167169Tetradecanoic acid, strontium salt (2:1)

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
50 °C

実験手順

100 of myristic acid which has been granulated from an aqueous emulsion as described in Example 1 (AN 246, titer 53° C. particle size 0.2-0.3 mm.) and 60.2 g strontium hydroxide octahydrate (97% active) are suspended in one liter of water at 50° C. temperature and stirred for 30 minutes at 50° C. followed by 60 minutes of agitation at 70° C. The hollow formed granulate is filtered and dried. The content of free fatty acid amounts to 1.7%.

後処理

  1. customtiter 53° C.
  2. waitfollowed by 60 minutes of agitation at 70° C
  3. filtrationThe hollow formed granulate is filtered
  4. customdried

出典と根拠

ORDレコード
ord-0e0c9f328fc14207a0f5b0bbce5340c2
出典データセット
uspto-grants-1980_11
特許番号
US04235794

関連ノート

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