化工社化工社 化学情報印刷レポート · 研究参考用
Stearic Acid → Lithium Stearate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Stearic Acid | HCID 5281 | — |
| 反応物 | Lithium hydroxide, monohydrate | HCID 168937 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Lithium Stearate | HCID 517357 | — |
反応手順
A suspension prepared from 55.0 g of granulated stearic acid (An 198, titer 66° C., particle size 100-300μ) and 8.1 g lithium hydroxide monohydrate in 550 ml of water is heated to 80° C. within 10-15 minutes. The remaining free fatty acid at this point is only 12.1%. Stirring is continued at 80° C. for the duration of one more hour and the resultant hollow granulate, which now contains only 0.4% free fatty acid, is filtered and dried.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04235794 |
| 出典データセット | uspto-grants-1980_11 |
| ORD ID | ord-8a93affccab648f2b29df974d1b87099 |
| 出典メモ | uspto-grants-1980_11 |