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3-Chloro-2-methylaniline → N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chloro-2-methylaniline | HCID 6894 | — |
| 反応物 | 4-Chlorobenzaldehyde | HCID 7726 | — |
| 生成物 | N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline | HCID 13017553 | — |
反応手順
2-methyl-3-chloroaniline (0.25 mole) and 4-chlorobenzaldehyde (0.25 mole) were ground in a mortar. The mixture was heated, with stirring in a water bath for 1.5 hours. Distillation at reduced pressure gave N-(p-chlorobenzylidene)-2-methyl-3-chloroaniline as a second fraction; B.p. 139° C./0.020 mm.; m.p. 79°-81° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04235929 |
| 出典データセット | uspto-grants-1980_11 |
| ORD ID | ord-f9d5df113c0a460b9c19606b5d3fecad |
| 出典メモ | uspto-grants-1980_11 |