化工社化工社 化学情報印刷レポート · 研究参考用
Binol → Toluene acetone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Binol | HCID 11762 | — |
| 反応物 | Iodide Ion | HCID 30165 | — |
| 触媒 | Silver bromoiodide | HCID 57465667 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Toluene acetone | HCID 20247278 | — |
反応手順
Three milliliters of this dispersion were added to a solution containing 0.3 millimoles (86 milligrams) of 1,1'-bi-2-naphthol (reducing agent) dissolved in 7 ml of a 2.0% by weight poly(vinyl butyral) solution in equal parts by volume acetone and toluene. 1.0 Milliliters of a photosensitive silver bromoiodide emulsion (6% iodide) in acetone and peptized with poly(vinyl butyral) was added to the resulting mixture with stirring.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04235957 |
| 出典データセット | uspto-grants-1980_11 |
| ORD ID | ord-00cdf01b60d8436eb373e4ee17e9c4fe |
| 出典メモ | uspto-grants-1980_11 |