関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dimethyl maleate | HCID 5271565 | — |
| 反応物 | Dimethylphosphite | HCID 21884954 | — |
| 溶媒 | Sodium Methoxide | HCID 10942334 | — |
| 生成物 | Dimethyl (dimethoxyphosphinyl)succinate | HCID 102330 | — |
反応手順
20 ml of 5% sodium methylate solution are added dropwise to 144 g (1 mol) of dimethyl maleate and 110 g of dimethyl phosphite until the exothermic reaction is completed. The reaction mixture is stirred for a further 30 minutes at 100° C. and then freed from low volatility constituents.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04235976 |
|---|
| 出典データセット | uspto-grants-1980_11 |
|---|
| ORD ID | ord-a86589083614466a91c3fab371711d9b |
|---|
| 出典メモ | uspto-grants-1980_11 |
|---|
