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Potassium periodate → Cis-1,4-Dimethoxy-9,10-dihydro-9,10-anthracenedicarboxaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium periodate | HCID 516896 | — |
| 反応物 | 1,4-Dimethoxy-9,10-dihydro-9,10-ethanoanthracene-11,12-diol | HCID 23329608 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Cis-1,4-Dimethoxy-9,10-dihydro-9,10-anthracenedicarboxaldehyde | HCID 88785356 | — |
反応手順
One gram of 1,4-dimethoxy-9,10-dihydro-9,10-ethanoanthracene-11,12-diol, is suspended in 30 ml. of an aqueous solution containing 0.77 g. of potassium periodate and one ml. of ethanol. After stirring at room temperature for 24 hours the insoluble material is removed by filtration, washed well with water and dried leaving a yellow product, m.p. 129°-132° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04235996 |
| 出典データセット | uspto-grants-1980_11 |
| ORD ID | ord-cb2cb3b108aa4d2da3ce5f436af99830 |
| 出典メモ | uspto-grants-1980_11 |