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HRID 225208作成日:2026年10月27日

Potassium periodate → Cis-1,4-Dimethoxy-9,10-dihydro-9,10-anthracenedicarboxaldehyde

https://huagongshe.com/reaction/225208

反応式

関与物質

役割名称HCID仕込み量
反応物Potassium periodateHCID 516896—
反応物1,4-Dimethoxy-9,10-dihydro-9,10-ethanoanthracene-11,12-diolHCID 23329608—
溶媒EthanolHCID 702—
生成物Cis-1,4-Dimethoxy-9,10-dihydro-9,10-anthracenedicarboxaldehydeHCID 88785356—

反応手順

One gram of 1,4-dimethoxy-9,10-dihydro-9,10-ethanoanthracene-11,12-diol, is suspended in 30 ml. of an aqueous solution containing 0.77 g. of potassium periodate and one ml. of ethanol. After stirring at room temperature for 24 hours the insoluble material is removed by filtration, washed well with water and dried leaving a yellow product, m.p. 129°-132° C.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04235996
出典データセットuspto-grants-1980_11
ORD IDord-cb2cb3b108aa4d2da3ce5f436af99830
出典メモuspto-grants-1980_11