化工社化工社 化学情報印刷レポート · 研究参考用
4'-Ethylacetophenone → 3-Dimethylamino-4'-ethylacrylophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4'-Ethylacetophenone | HCID 13642 | — |
| 反応物 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 生成物 | 3-Dimethylamino-4'-ethylacrylophenone | HCID 53833899 | — |
反応手順
A mixture of 50 g. of 4'-ethylacetophenone and 50 ml. of dimethylformamide dimethylacetal is refluxed for 16 hours. Evaporation gave a thick oil which crystallized on the addition of hexane, m.p. 80°-81° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04236005 |
| 出典データセット | uspto-grants-1980_11 |
| ORD ID | ord-c7547d413d064fea83690359d7aa349b |
| 出典メモ | uspto-grants-1980_11 |