1-Benzyl-4-ethylpyridinium chloride → Benzyl Chloride
反応式
[Cl-:1].[C:2]1([CH2:8][N+:9]2[CH:14]=[CH:13][C:12]([CH2:15][CH3:16])=[CH:11][CH:10]=2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C(O)(C)C>[CH2:15]([C:12]1[CH:13]=[CH:14][N:9]=[CH:10][CH:11]=1)[CH3:16].[CH2:8]([Cl:1])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
4
実験手順
Following a procedure similar to that described in Example 1(a), 415 g (89%) of N-(phenylmethyl)-4-ethylpyridinium chloride obtained from 4-ethylpyridine (214 g, 2.0 mol), benzyl chloride (253 g, 2.0 mol) and isopropanol (1200 mL). The product had a melting point of 157°-162° C.
出典と根拠
- ORDレコード
- ord-dd6315e7d5af4c069d9767734a63fafb
- 出典データセット
- uspto-grants-1993_08
- 特許番号
- US05240935
反応ノート
読み込み中…