Butyric Acid → HCID 10851091、化合物

反応式

[C:1]([C:5]1[C:10]2[S:11][CH2:12][C:13]([CH3:15])([CH3:14])[C:9]=2[CH:8]=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[C:16](O)(=[O:20])[CH2:17][CH2:18][CH3:19]>>[C:1]([C:5]1[C:10]2[S:11][CH2:12][C:13]([CH3:15])([CH3:14])[C:9]=2[CH:8]=[C:7]([C:16](=[O:20])[CH2:17][CH2:18][CH3:19])[CH:6]=1)([CH3:4])([CH3:2])[CH3:3]

参加物

反応物 2

HCID 264Butyric Acid

HCID 107041827-tert-butyl-2,3-dihydro-3,3-dimethylbenzothiophene

生成物 1

HCID 10851091HCID 10851091、化合物

実験手順

Substantially the method described in Example 1 is employed for the reaction between 7-tert-butyl-3,3-dimethyl-2,3-dihydrobenzo[b]thiophene and butanoic acid, to provide 1-(7-tert-butyl-3,3-dimethyl-2,3-dihydrobenzo[b]thiophen-5-yl)-butan-1-one as a colorless oil.

出典と根拠

ORDレコード: ord-9c4aefe4e535490895b6ba0ef0f8fca9
出典データセット: uspto-grants-1997_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05656661

反応ノート

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