化工社化工社 化学情報印刷レポート · 研究参考用
1,3-Benzothiazole-6-sulfonyl chloride → N-(2-Bromo-6-methyl-3-pyridyl)-6-benzothiazolesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,3-Benzothiazole-6-sulfonyl chloride | HCID 2795170 | — |
| 反応物 | 2-Bromo-6-methylpyridin-3-amine | HCID 14418051 | — |
| 生成物 | N-(2-Bromo-6-methyl-3-pyridyl)-6-benzothiazolesulfonamide | HCID 86622569 | 35% |
反応手順
By working in a manner similar to that of Preparation VII, starting with 3-amino-2-bromo-6-methylpyridine and 6-benzothiazolesulfonyl chloride, the expected product is obtained in the form of a beige-colored paste (yield=35%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07557122B2 |
| 出典データセット | uspto-grants-2009_07 |
| ORD ID | ord-a57f06a4edee43388913997c8df6648f |
| 出典メモ | uspto-grants-2009_07 |