O-Xylene → HCID 18788042、化合物

HRID 2258381

反応式

HRID 2258381 の反応式
[CH2:1]([N:5](CC(C)=C)[C:6]1[CH:11]=CC=C[CH:7]=1)[CH2:2][CH2:3][CH3:4].[C:16]1([CH3:23])[C:17](C)=[CH:18][CH:19]=[CH:20][CH:21]=1>[Cl-].[Zn+2].[Cl-]>[CH2:1]([N:5]1[C:17]2[C:16](=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:23][C:6]1([CH3:11])[CH3:7])[CH2:2][CH2:3][CH3:4]

参加物

4

反応物 2

HCID 7237O-XyleneHCID 54010992N-butyl-N-(2-methylprop-2-eneyl)aniline

生成物 1

HCID 18788042HCID 18788042、化合物

試薬・触媒・溶媒 1

HCID 3007855Zincchloride触媒

実験手順

A mixture of N-butyl-N-(2-methylprop-2-eneyl)aniline (9.6 parts), zinc chloride (6.12 parts) and xylene (20 parts) was heated under reflux with vigorous stirring for 4.75 hours. The cooled mixture was filtered and the organic phase evaporated to leave 1-butyl-2,2-dimethylindoline (5.3 parts).

後処理

  1. temperaturewas heated
  2. temperatureunder reflux
  3. filtrationThe cooled mixture was filtered
  4. customthe organic phase evaporated

出典と根拠

ORDレコード
ord-7f603290ea884b37aa05920e12f26970
出典データセット
uspto-grants-1997_08
特許番号
US05660598

関連ノート

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