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Isophthalaldehyde → 3-(2-(7-Chloroquinolin-2-yl)vinyl)benzaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isophthalaldehyde | HCID 34777 | — |
| 反応物 | 7-Chloro-2-methylquinoline | HCID 138395 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 溶媒 | Acetic Anhydride | HCID 7918 | — |
| 生成物 | 3-(2-(7-Chloroquinolin-2-yl)vinyl)benzaldehyde | HCID 53394853 | — |
反応手順
A solution of isophthalaldehyde (4.0 g) and 7-chloroquinaldine (5.39 g) in acetic anhydride was heated at 125° in an oil bath for 48 hours. The reaction was cooled to room temperature, diluted with ether (30 mL) and the resulting suspension was stirred vigorously. The solid title compound was collected by filtration and was used as such in the next step.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05428171 |
| 出典データセット | uspto-grants-1995_06 |
| ORD ID | ord-82aa24b70650476f8934154e035255ed |
| 出典メモ | uspto-grants-1995_06 |