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Potassium Hydroxide → N-(2,3-dihydroxypropyl)-N-hexadecyl-2-hydroxyhexadecanamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | 3-(Hexadecylamino)propane-1,2-diol | HCID 111007 | — |
| 反応物 | Methyl 2-hydroxyhexadecanoate | HCID 543716 | — |
| 生成物 | N-(2,3-dihydroxypropyl)-N-hexadecyl-2-hydroxyhexadecanamide | HCID 15825476 | — |
反応手順
N-(2,3-dihydroxypropyl)-N-hexadecylamine (1.0 g, 0.0032 mole) and potassium hydroxide (0.01 g, 0.18 mmole) were heated to 85° C. under vacuum and methyl 2-hydroxyhexadecanoate (0.907 g, 0.0032 mole) was heated and added dropwise to the reaction. The reaction was heated under vacuum for 6 hours. A waxy off-white solid was obtained (crude yield=1.79 g). The waxy solid was recrystalized from hot hexane (yield=0.94 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05476671 |
| 出典データセット | uspto-grants-1995_12 |
| ORD ID | ord-b95a455865cc49fc8505d782444943a7 |
| 出典メモ | uspto-grants-1995_12 |