化工社化工社 化学情報印刷レポート · 研究参考用
Diisopropylaniline → Dibenz(b,e)oxepin-11-carboxamide, 6,11-dihydro-N-(2,6-bis(1-methylethyl)phenyl)-2-methyl-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diisopropylaniline | HCID 32484 | — |
| 反応物 | 6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid | HCID 10106342 | — |
| 生成物 | Dibenz(b,e)oxepin-11-carboxamide, 6,11-dihydro-N-(2,6-bis(1-methylethyl)phenyl)-2-methyl- | HCID 3072807 | 94.8% |
反応手順
The similar procedures as in Example 1 were repeated except using 1.20 g of Compound A and 1.00 g of 2,6-diisopropylaniline in place of aniline to obtain 1.85 g of Compound 4.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05478835 |
| 出典データセット | uspto-grants-1995_12 |
| ORD ID | ord-331cf4583d0546198a0894dcfb6724b2 |
| 出典メモ | uspto-grants-1995_12 |